Journal
JOURNAL OF PHYSICS AND CHEMISTRY OF SOLIDS
Volume 69, Issue 5-6, Pages 1454-1456Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.jpcs.2007.10.134
Keywords
oxides; crystal growth; x-ray diffraction; crystal structure
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Single crystal of Li4Ti5O12 was synthesized by a flux method using LiCl flux. The obtained Li4Ti5O12 single crystal is colorless and has the shape of a rod. Li4Ti5O12 crystallizes in the cubic spinel type structure, space group Fd (3) over barm, a = 8.352 (4)angstrom, V = 583.6 (8) angstrom(3), and Z = 8. The structure was determined by a single-crystal X-ray study and refined to the conventional values of R 3.6% and wR = 3.3% for 209 independent observed reflections. (c) 2007 Elsevier Ltd. All rights reserved.
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