Journal
JOURNAL OF PHYSICAL CHEMISTRY LETTERS
Volume 3, Issue 15, Pages 2030-2034Publisher
AMER CHEMICAL SOC
DOI: 10.1021/jz300742w
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Funding
- National Institute of Biomedical Imaging and Bioengineering of the National Institute of Health [EB-001960, EB-002804, EB-00103S, EB-002026]
- Natural Sciences and Engineering Research Council of Canada
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Oxygen-17-detected DNP NMR of a water/glycerol glass enabled an 80-fold enhancement of signal intensity at 82 K, using the biradical TOTAPOL. The >6000-fold savings in acquisition time enable O-17-H-1 distance measurements and heteronuclear correlation experiments. These experiments are the initial demonstration of the feasibility of DNP NMR on quadrupolar O-17.
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