Journal
JOURNAL OF PHYSICAL CHEMISTRY C
Volume 114, Issue 6, Pages 2640-2644Publisher
AMER CHEMICAL SOC
DOI: 10.1021/jp908939e
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Funding
- University of Chicago [DE-AC02-06CH 11357]
- Argonne
- LLC
- Argonne National Laboratory
- U.S. Department of Energy
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A carbon fiber microelectrode (CFME) was used for characterization of the nanoparticle catalysts as an alternative to the well-established rotating disk electrode (RDE) method. We found that the novel CFME method yielded comparable results to the RDE method when investigating the adsorption/desorption processes as well the specific activity for reactions such as the oxygen reduction reaction. Its major advantage over the RDE method is a fast sample preparation and rapid measurement, reducing significantly the time of a single sample characterization from 2-3 h to a favorable 5-10 min.
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