Journal
JOURNAL OF ORGANOMETALLIC CHEMISTRY
Volume 693, Issue 21-22, Pages 3425-3429Publisher
ELSEVIER SCIENCE SA
DOI: 10.1016/j.jorganchem.2008.08.007
Keywords
cyclotetramerization; metallophthalocyanine; synthesis; microwave; 1,2,4-triazole
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Funding
- Karadeniz Technical University, Trabzon, Turkey
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The synthesis of metallophthalocyanines [6-9; M = Ni(II), Zn(II), Co(II) and Cu(II)] with four 1,2,4-triazole units obtained from 4-{(4-chloro-2-fluorobenzyl)[3-(4-chlorophenyl)-5-(4-methylphenyl)-4H-1,2,4-triazol-4-yl] amino} phthalonitrile (5) in the presence of dimethylaminoethanol and the corresponding anhydrous metal salts is described. The thermal stabilities of the Pc compounds were determined by thermogravimetric analysis. The new compounds were characterized by a combination of IR, H-1 NMR, C-13 NMR, UV-Vis, elemental analysis. (C) 2008 Elsevier B.V. All rights reserved.
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