Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 79, Issue 20, Pages 9613-9618Publisher
AMER CHEMICAL SOC
DOI: 10.1021/jo501736w
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Funding
- National Natural Science Foundation of China [21272021]
- National Key Technology RD Program [2011BAD23B01]
- Beijing City Education Committee [KM201010005009]
- U.S. National Science Foundation
- Office Of Internatl Science &Engineering
- Office Of The Director [0968399] Funding Source: National Science Foundation
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An electrochemically promoted coupling of benzoxazoles and amines has been developed, leading directly to the formation of 2-aminobenzoxazoles. The chemistry utilizes catalytic quantities of a tetraalkylammonium halide redox catalyst and is carried out under constant current conditions in a simple undivided cell. The use of excess chemical oxidant or large amounts of supporting electrolyte is avoided. This greatly simplifies the workup and isolation process and leads to a reduction in waste.
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