Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 79, Issue 7, Pages 2955-2962Publisher
AMER CHEMICAL SOC
DOI: 10.1021/jo5000219
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Funding
- NSF of China [21102133, 21172200]
- NSF of Henan [082300423201]
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A highly efficient and practical procedure to acylazobenzene via Pd-catalyzed oxidative C-H bond activation from toluene has been developed. Various mono- and diacylazobenzene were afforded simultaneously in moderate to excellent yields for 33 examples. Toluene and its derivatives were served as potential and ideal acylation reagents. The mono- and diacylated products could be controlled by the oxidant loading.
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