4.7 Article

A Metal-Free Tandem C-C/C-O Bond Formation Approach to Diversely Functionalized Tetrasubstituted Furans

Journal

JOURNAL OF ORGANIC CHEMISTRY
Volume 79, Issue 1, Pages 106-116

Publisher

AMER CHEMICAL SOC
DOI: 10.1021/jo4023342

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Funding

  1. CSIR, New Delhi [CSC-108]

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A novel and efficient method for the synthesis of diversely functionalized furans is developed via DBU-mediated tandem Michael addition/5-exo-dig-cycloisomerization of enynes and keto-methylenes. This [3 + 2]-annulation is operationally simple under metal-free reaction conditions with 100% atom economy and broad substrate scope.

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