Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 78, Issue 12, Pages 6202-6210Publisher
AMER CHEMICAL SOC
DOI: 10.1021/jo4008892
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Funding
- MEXT [20675002]
- ACT-C from JST (Japan)
- Grants-in-Aid for Scientific Research [25105714] Funding Source: KAKEN
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The convenient synthesis of substituted triphenylenes and azatriphenylenes has been achieved by the cationic rhodium(I)/H-8-BINAP or BINAP complex-catalyzed [2 + 2 + 2] cycloaddition under mild conditions. Photo-physical properties of representative triphenylenes and azatriphenylenes were examined, which revealed that azatriphenylenes showed higher fluorescence quantum yields than triphenylenes. This method was successfully applied to the synthesis of highly fluorescent triphenylene-based long ladder molecules.
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