Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 78, Issue 3, Pages 1236-1241Publisher
AMER CHEMICAL SOC
DOI: 10.1021/jo3024686
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Funding
- National Basic Research Program (973 program) [2009CB825300]
- Natural Science Foundation of China [21272010]
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A CuI-catalyzed synthesis of 1,3-disubstituted allenes from 1-alkynes by the reaction with various N-tosylhydrazones has been developed. This method, which uses readily available starting materials and is operationally simple, offers 1,3-disubstituted allenes in moderate to good yields. The reaction also tolerates various functional groups.
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