Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 78, Issue 18, Pages 9517-9521Publisher
AMER CHEMICAL SOC
DOI: 10.1021/jo4016612
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Funding
- EPSRC
- GSK Ltd.
- EPSRC [EP/D072182/1] Funding Source: UKRI
- Engineering and Physical Sciences Research Council [EP/D072182/1] Funding Source: researchfish
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Tetramethylethylenediamine (TMEDA) acts as cheap and readily removed ligand in the iron-catalyzed coupling of alkyl Grignard reagents and activated aryl chlorides. The use of TMEDA allows for low ligand and iron catalyst loading as well as an increased reaction concentration and an ambient reaction temperature on a mole scale.
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