Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 78, Issue 4, Pages 1463-1470Publisher
AMER CHEMICAL SOC
DOI: 10.1021/jo302534f
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- DST (New Delhi)
- UGC under UPE
- UGC under CAS
- CSIR (New Delhi)
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Copper bromide promoted reactions of aldehydes, 1-alkynes, and chiral 2-dialkylaminomethylpyrrolidine at 25 degrees C give the corresponding chiral propargylamine derivatives in up to 96% yield and 99:1 dr that are readily converted to the corresponding disubstitued chiral allenes in up to 81% yield and 99% ee upon reaction with CuI in dioxane at 100 degrees C.
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