Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 78, Issue 12, Pages 6328-6331Publisher
AMER CHEMICAL SOC
DOI: 10.1021/jo4008157
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Funding
- Basic Science Research Program through the National Research Foundation of Korea (NRF)
- Ministry of Education, Science and Technology [2010-0021923]
- Kwangwoon University
- National Research Foundation of Korea [2010-0021923] Funding Source: Korea Institute of Science & Technology Information (KISTI), National Science & Technology Information Service (NTIS)
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Although a number of methods have been developed to reduce sulfoxides to sulfides, many of these processes are limited by side reactions, low yields, poorly available reagents, or harsh reaction conditions. We recently studied the reaction of various sulfoxides with SOCl2 and Ph3P. We were able to obtain the corresponding sulfides in excellent yields (>90%) when aliphatic and aromatic sulfoxides were treated with SOCl2 as a catalyst and Ph3P in THF at room temperature.
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