Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 78, Issue 8, Pages 3847-3857Publisher
AMER CHEMICAL SOC
DOI: 10.1021/jo400263w
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Funding
- JSPS [22249001, 21790019]
- MEXT [2304, 24105526, 2105, 24106736]
- Research Foundation for Pharmaceutical Sciences
- Grants-in-Aid for Scientific Research [22249001, 24659009, 24106736, 25253002, 24105526, 21790019] Funding Source: KAKEN
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The stereocontrolled total synthesis of (-)-cinatrin C-1, a phospholipase A(2) inhibitor, has been accomplished. The key feature includes the stereoselective construction of the highly substituted tetrahydrofuran core by In(OTf)(3)-catalyzed Conia-ene reaction of the oxygen-tethered acetylenic malonic ester followed by dihydroxylation with concomitant lactonization.
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