Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 78, Issue 6, Pages 2751-2756Publisher
AMER CHEMICAL SOC
DOI: 10.1021/jo302676g
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Funding
- DFG [NA 955/1-1]
- Fonds der Chemischen Industrie (Sachkostenzuschuss)
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An iodocyclization reaction of o-alkynylphenyl carboxaldehydes is reported that is truly catalytic with respect to the electrophilic iodine source. With a combination of tetrabutylammonium iodide (TBAI), Oxone as non-nucleophilic and easy to handle co-oxidant, and fluorinated protic solvents, highly substituted 1-naphthalenones could be prepared in high yields of up to 91%.
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