Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 77, Issue 20, Pages 9379-9383Publisher
AMER CHEMICAL SOC
DOI: 10.1021/jo3015819
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- CSIR, New Delhi [01(2365/10/EMR-II)]
- CSIR
- Nanoscience Project Unit at IACS
- DST, New Delhi
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An efficient Sonogashira coupling of terminal alkynes and styrenyl bromides has been achieved under the catalysis of hydroxyapatite-supported copper(I). The trans-styrenyl bromides produce the usual trans-enyne products, whereas the cis-styrenyl bromides lead to unsymmetric 1,3-diynes by the cross coupling of terminal alkyne and the alkyne generated from the cis-styrenyl bromide. A series of trans-enynes and unsymmetric 1,3-diynes have been synthesized by this protocol.
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