Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 78, Issue 1, Pages 204-210Publisher
AMER CHEMICAL SOC
DOI: 10.1021/jo302230m
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Funding
- NIH [HL25848]
- NSF
- Weill Cornell Medical School for an NIH postdoctoral fellowship [CA062948]
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Halocycloalkenones are demonstrated to function as potent dienophiles in inter- and intramolecular Diels Alder cydoadditions. We have found 2-brominated cycloalkenone dienophiles to be both highly endo selective and significantly more reactive than their nonhalogenated parent compounds. A method for the facile conversion of brominated cyclobutanone DA adducts to synthetically useful cydopropyl functional handles is described.
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