Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 77, Issue 22, Pages 10455-10460Publisher
AMER CHEMICAL SOC
DOI: 10.1021/jo3019939
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Funding
- Department of Science and Technology, New Delhi [SR/S1/OC-25/2008]
- Council of Scientific and Industrial Research (CSIR) New Delhi
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A general, efficient, and common strategy for the synthesis of (-)-juglomycin A, (+)-kalafungin, (+)-frenolicin B, and (+)-deoxyfrenolicin is reported here. The strategy involves the synthesis of a key building block alkyne from a cheap chiral pool material, D-glucono-delta-lactone, Dotz benzannulation, oxa-Pictet-Spengler reaction, and H2SO4-mediated epimerization.
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