Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 76, Issue 8, Pages 2613-2618Publisher
AMER CHEMICAL SOC
DOI: 10.1021/jo1024927
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Funding
- VEGA [1/0340/10]
- Slovak Academic Information Agency (Action Austria-Slovakia)
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A tandem catalysis protocol based on decarboxylative coupling of alkynoic acids and 1,3-dipolar cycloaddition of azides enables a highly efficient synthesis of a variety of functionalized 1,2,3-triazoles. The three-step, one-pot method avoids usage of gaseous or highly volatile terminal alkynes, reduces handling of potentially unstable and explosive azides to a minimum, and furnishes target structures in excellent yields and a very good purity without the need for additional purification.
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