Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 76, Issue 22, Pages 9329-9337Publisher
AMER CHEMICAL SOC
DOI: 10.1021/jo2015906
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Funding
- National Natural Science Foundation of China [20872127, 20732005, J0830431]
- National Basic Research Program of China (973 Program) [2009CB825300]
- CAS Academician Foundation of Zhejiang Province
- Fundamental Research Funds for the Central Universities
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The manganese(III) acetate-mediated free radical cyclization of diarylmethylenecyclopropa[b] naphthalenes with nucleophiles such as carboxylic acid and sulfonic acid provides an efficient method for the synthesis of 1,2-benzanthracenes in moderate to good yields under mild conditions. In addition, after several steps of simple and routine operations, the obtained 1,2-benzanthracenes bearing an acetoxy group could be easily converted to structurally more sophisticated 1,2-benzanthracene derivatives, which are not easily accessible yet potentially useful candidates for materials science.
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