Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 76, Issue 21, Pages 9109-9115Publisher
AMER CHEMICAL SOC
DOI: 10.1021/jo201334n
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Funding
- National Sciences Foundation of China [20972155]
- National Basic Research Program of China (973 Program) [2010CB833300]
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Enantioselective synthesis of 4-substituted 4,5-dihydro-1H-[1,5]benzodiazepin-2(3H)-ones has been accomplished through chiral Lewis base-catalyzed hydrosilylation. The corresponding products were obtained in excellent yields (up to 99%) and enantioselectivities (up to 98%). The absolute configuration of product 3n has been determined as S by X-ray crystallographic analysis.
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