Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 76, Issue 5, Pages 1444-1447Publisher
AMER CHEMICAL SOC
DOI: 10.1021/jo102062u
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Funding
- Chinese Academy of Sciences [KGCXZ-YW-389]
- National Science Foundation of China [20732007, 21090343, 50973125]
- Ministry of Science and Technology of China [G2007CB808004, 2009CB220008]
- Bureau for Basic Research of the Chinese Academy of Sciences
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With visible light irradiation (lambda > 400 nm) of rhenium(I) complexes (P1-P4), a photochemical conversion from 3,4-dihydropyrimidin-2(1H)-ones to pyrimidin-2(1H)-ones at room temperature has been achieved with good to excellent yields in CH3CN-H2O solution containing CCl4 and K2CO3. Luminescence quenching study and product analysis reveal that photoinduced electron transfer between rhenium(I) complex P and 3,4-dihydropyrimidin-2(1H)-ones plays an important role in the initial event.
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