Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 76, Issue 8, Pages 2875-2879Publisher
AMER CHEMICAL SOC
DOI: 10.1021/jo200137k
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Funding
- University of Iowa
- Roy J. Carver Charitable Trust
- National Institutes of Health [DA02-6573]
- Direct For Mathematical & Physical Scien
- Division Of Chemistry [0946779] Funding Source: National Science Foundation
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Benzyl phosphonate esters often serve as reagents in Horner-Wadsworth-Emmons reactions. In most cases, they can be prepared from benzylic alcohols via formation of the corresponding halide followed by an Arbuzov reaction. To identify a more direct synthesis of phosphonate esters, we have developed a one-flask procedure for conversion of benzylic and allylic alcohols to the corresponding phosphonates through treatment with triethyl phosphite and ZnI2.
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