Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 76, Issue 22, Pages 9507-9513Publisher
AMER CHEMICAL SOC
DOI: 10.1021/jo2017108
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Funding
- Fundamental Research Funds for the Central Universities [DL12DB03, DL10BB07]
- China Postdoctoral Science Foundation [20110491013]
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The palladium-catalyzed intramolecular C-H activation/C-C cross-coupling has been developed for a straightforward and efficient synthesis of phenanthridines. With Pd(OAc)(2) (4 mol %) as the catalyst, PCy3 (8 mol %) as the ligand, and Cs2CO3 as the base, this protocol was applied to synthesize a small library of phenanthridine derivatives in good yields in THF.
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