Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 76, Issue 19, Pages 7945-7952Publisher
AMER CHEMICAL SOC
DOI: 10.1021/jo2013669
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Funding
- US Army [PC073739]
- NIH/NIAID [AI074461]
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The syntheses of the natural product anibamine and its three olefin isomers have been achieved concisely and efficiently via highly regio- and stereoselective reactions. The crucial steps included a regioselective palladium-catalyzed alkynylation by Sonogashira coupling and a stereoselective Suzuki coupling. Further conformation analyses and in vitro calcium mobilization studies were carried out to characterize the compounds' biological properties.
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