Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 75, Issue 24, Pages 8677-8680Publisher
AMER CHEMICAL SOC
DOI: 10.1021/jo101640z
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Funding
- National Natural Science Foundation of China [20872128, J0830413]
- Fundamental Research Funds for the Central Universities [2009QNA3011]
- Natural Science Foundation of Zhejiang Province [R407106]
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A new class of chiral phosphoric acids with spirobiindane s scaffold were conveniently synthesized from (S)-1,1'-spirobiindane-7,7'-diol ((S)-SPINOL) and employed to catalyze the asymmetric Friedel-Crafts reaction of in-doles with imines to afford 3-indolylmethanamines. High yields (68-97%) and excellent enantioselectivities (up to 99% ee) were obtained.
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