Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 75, Issue 13, Pages 4644-4647Publisher
AMER CHEMICAL SOC
DOI: 10.1021/jo1008178
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Double glycosylation of cysteine-containing peptides has been carried out by a one-pot two-step sequence comprising selective S-propargylation followed by photoinduced, (lambda(max) 365 nm) free-radical hydrothiolation with glycosyl thiols. Conditions were established for the sequential introduction of two different thiol residues such as a glycosyl and a biotinyl derivative.
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