Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 75, Issue 15, Pages 5355-5358Publisher
AMER CHEMICAL SOC
DOI: 10.1021/jo100867v
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Funding
- National Science Foundation [0846756]
- Direct For Mathematical & Physical Scien
- Division Of Chemistry [0846756] Funding Source: National Science Foundation
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We are reporting the first total synthesis of the tetracyclic terpene natural product cryptoacetalide. Key steps of the synthesis are a microwave-mediated [2+2+2] cyclotrimerization reaction to construct the central benzene ring, and a light-mediated radical cyclization to assemble the spiro-ketal moiety.
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