Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 75, Issue 13, Pages 4612-4614Publisher
AMER CHEMICAL SOC
DOI: 10.1021/jo100468s
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- Landesgraduiertenforderung Baden-Wurttemberg
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4-Hydroxy[2.2]paracyclophane is readily prepared via an improved synthetic protocol from unsubstituted[2.2]paracyclophane. The key step is a Dakin oxidation of 4-formyl[2.2]paracyclophane. This allows a rapid access to large quantities of the product and an easy synthesis of the enantiopure form.
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