Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 74, Issue 16, Pages 6358-6361Publisher
AMER CHEMICAL SOC
DOI: 10.1021/jo901065y
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Funding
- Korea Research Foundation
- Korean Government (MOEHRD, Basic Research Promotion Fund) [KRF-2008-314-D00070]
- National Research Foundation of Korea [과C6A1901, 314-2008-1-D00070, 과06B1512] Funding Source: Korea Institute of Science & Technology Information (KISTI), National Science & Technology Information Service (NTIS)
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Nickel-catalyzed aminocarbonylation of aryl halides is described. A well-defined air-stable nickel-phosphite catalytic system (Ni(OAc)(2)center dot 4H(2)O/phosphite 1) effectively promoted the aminocarbonylation of aryl bromides with a range of formamides to give the corresponding aryl amide products in moderate to good yields. The less hindered formamide required lower catalytic loading for full conversion and produced higher yields than the more hindered one. It also exhibited base-dependent activity toward formamides.
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