Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 74, Issue 2, Pages 899-902Publisher
AMER CHEMICAL SOC
DOI: 10.1021/jo802318p
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Funding
- Department of Science and Technology of Jilin Province [20080421]
- [NENU-STB07007]
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p-Terphenyls and heteroaryl analogues including bipyridines were prepared via [5C + 1C(N)] annulation of alpha-aryl-alpha-alkenoyl ketene-(S,S)-acetals (five carbon 1,5-bielectrophilic species) with nitroethane or ammonium acetate, The reaction features mild conditions, multisubstitution, and functional group tolerance and is metal catalyst free. The present protocol provides, a new alternative to the conventional methodologies for the synthesis of teraryls.
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