Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 74, Issue 21, Pages 8373-8376Publisher
AMER CHEMICAL SOC
DOI: 10.1021/jo9015985
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Calcium D-glucarate was converted into D-glucaro-1,4:6,3-dilactone on 32-g, 1-kg, and 22-kg scale, using azeotropic distillation with methyl isobutyl ketone to drive the dehydration. The crystalline product was >= 99.5% pure by GC and NMR, and overall yield was its high as 72%.
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