Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 74, Issue 20, Pages 7844-7848Publisher
AMER CHEMICAL SOC
DOI: 10.1021/jo9016309
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Funding
- National Natural Science Foundation of China [20872112]
- Zhejiang Provincial Natural Science Foundation of China [Y407116, Y4080169]
- Wenzhou University [2007L004]
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An efficient synthesis of 3-chalcogen-benzo[b]furans via palladium-promoted annulation reactions of 2-alkynylphenol derivatives with disulfides or diselenides and iodide has been developed. In the presence of I-2 and PdCl2, both 3-sulfenylbenzofurans and 3-selenenylbenzofurans were selectively prepared from the cyclization of 2-alkynyanisoles with disulfides or diselenides in moderate to excellent yields.
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