Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 73, Issue 2, Pages 772-774Publisher
AMER CHEMICAL SOC
DOI: 10.1021/jo702409y
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[GRAPHICS] We have developed a convenient method for the efficient monofluorination via the electrophilic fluorocyclization reaction of 2,3-allenoic acids with Selectfluor in MeCN in the presence of 10 equiv of H2O or even in pure water to afford beta-fluorobutenolides in moderate to high yields.
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