Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 73, Issue 9, Pages 3608-3611Publisher
AMER CHEMICAL SOC
DOI: 10.1021/jo702573z
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A practical and efficient synthesis of spirobarbiturates of type III is reported when NH acidity of the imide function of the hydrophilic linker element allowed the introduction of different substituents. Structural characterization, which was based on both X-ray crystallography and spectroscopic linvestigations, indicated type II beta-turn formation. Introduction of the molecular scaffold into solid phase peptide synthesis gave rise to spirocyclic neuropeptide analogs.
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