Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 73, Issue 5, Pages 1946-1953Publisher
AMER CHEMICAL SOC
DOI: 10.1021/jo702620e
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[GRAPHICS] A stepwise [3 + 3] annelation reaction has been developed that allows access to pyrans from epoxides. This process involves the addition of an allylmagnesium reagent, itself readily prepared from methallyl alcohol, and a Pd-catalyzed cyclodehydration reaction. The potential of this process to be employed in natural product synthesis has been exemplified by its use in the preparation of rhopaloic acid A.
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