Journal
JOURNAL OF NATURAL PRODUCTS
Volume 74, Issue 1, Pages 69-73Publisher
AMER CHEMICAL SOC
DOI: 10.1021/np100710c
Keywords
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Funding
- NZ Foundation for Research, Science & Technology (FRST)
- Cancer Society of New Zealand
- Curtis-Gordon Research Scholarship in Chemistry (VUW)
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Examination of the New Zealand sponge Raspailia agminata resulted in the isolation of five members of a novel family of glycolipids, agminosides A-E (1-5). These large and complex molecules contain up to six partially acetylated glucose residues. The chromatographic separation of these compounds was a challenge due to the similarity of the congeners and their lack of a chromophore. MS-guided isolation followed by extensive NMR analysis and chemical derivatization eventually led to the purification and identification of 1-5.
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