Journal
JOURNAL OF NATURAL PRODUCTS
Volume 74, Issue 3, Pages 430-440Publisher
AMER CHEMICAL SOC
DOI: 10.1021/np1008637
Keywords
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Funding
- NSF [OCE-0095724, 0550468, CHE0741968]
- NIH [CA122256, AI039987]
- Ruth L. Kirschstein National Research Service [T32 CA009523]
- Direct For Mathematical & Physical Scien
- Division Of Chemistry [0741968] Funding Source: National Science Foundation
- Office of Polar Programs (OPP)
- Directorate For Geosciences [0550468] Funding Source: National Science Foundation
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The complete stereostructures of xestoproxamines A-C, from the Bahamian sponge Neopetrosia proxima, were assigned from spectroscopic analysis, including MS, 2D NMR, and integrated degradation-CD analysis. Two new CD application protocols are described for defining absolute configuration: one for allylic methyl groups in branched chains and a second for the heterocyclic core bis-piperidine with Specific applicability to other members of this class alkaloids-known for their stereoheterogeneity-and tertiary cyclic amines in general.
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