Journal
JOURNAL OF MOLECULAR STRUCTURE
Volume 1013, Issue -, Pages 138-142Publisher
ELSEVIER SCIENCE BV
DOI: 10.1016/j.molstruc.2012.01.022
Keywords
Crystal structure; Methyl orange ligand; Spectroscopic analysis; Acid-base indicator
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The first example of cadmium complex containing methyl orange [MO, (CH3)(2)NC6H4N = NC6H4SO3Na], formulated as [Cd(en)(2)(H2O)(2)](MO)(2) 1 (en = ethylenediamine) was synthesized hydrothermally and characterized by single-crystal X-ray diffraction, IR, XRD, elemental analysis and Raman spectroscopic analysis. Compound 1 display a two-dimensional supramolecular layer structure with ladder-like supramolecular chain by X-ray crystallographic analysis. MO anion immobilized by H-bonds, as acid-base indicator, shows a similar behavior in comparison with its solution counterpart in terms of response to pH. (C) 2012 Elsevier B.V. All rights reserved.
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