Journal
JOURNAL OF MOLECULAR CATALYSIS A-CHEMICAL
Volume 395, Issue -, Pages 217-224Publisher
ELSEVIER
DOI: 10.1016/j.molcata.2014.08.027
Keywords
Azetidines; Ring opening; Hydrogenolysis; Palladium; Solvent effects
Categories
Funding
- Hungarian Scientific Research Fund [OTKA K104528]
- New Hungary Development Plan [TAMOP-4.2.1/B-09/1/KMR-2010-0002]
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Some N- and O-protected hydroxyazetidine derivatives were hydrogenated to the corresponding amines or aminoalcohols over a Pd/C catalyst, in different solvents (methanol, dichloromethane, tetrahydrofuran), at 30-60 degrees C and 1-10 bar. These amino compounds, formed during hydrogenolytic ring opening and/or deprotecting reactions, are potential starting materials for preparing optically active, practically important pyrrolidine derivatives. (C) 2014 Elsevier B.V. All rights reserved.
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