Journal
JOURNAL OF MATERIALS SCIENCE-MATERIALS IN ELECTRONICS
Volume 24, Issue 7, Pages 2485-2492Publisher
SPRINGER
DOI: 10.1007/s10854-013-1122-5
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Funding
- Office of Graduate Studies of the University of Isfahan
- Iranian Nanotechnology Initiative Council
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Ultra-fine nanoparticles of strontium hexaferrite, SrFe12O19, have been synthesized by low-temperature solid-state reaction method without ball-milling process. The effects of the preparing conditions of samples such as calcination temperature, Fe3+/Sr-2 and Na1+/Sr2+ mole ratio on the phase composition, particle size and shape and magnetic properties of the calcined samples have been investigated by differential thermal analysis, X-ray diffraction, field emission scanning electronic microscopy, and vibrating sample magnetometery. The X-ray diffraction patterns showed the formation of SrFe12O19 single phase at temperatures as low as 750 degrees C. Fine particles with particle size around 30-100 nm obtained at 750 degrees C with Fe3+/Sr-2 mole ratio of 10. The magnetic measurements and structural analysis showed that particles were single domain and exhibited better magnetic properties than those obtained by the ceramic method.
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