Journal
JOURNAL OF MATERIALS SCIENCE & TECHNOLOGY
Volume 27, Issue 3, Pages 245-251Publisher
JOURNAL MATER SCI TECHNOL
DOI: 10.1016/S1005-0302(11)60057-1
Keywords
Carbon nitride materials; Solid state reactions; Intercalation; Microstructure
Funding
- shandong Science and Technology Council, China [BS2010CL013]
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Graphite-like carbon nitride (g-C3N4) was synthesized in large quantities at 300 degrees C under nitrogen by a solid-state reaction route. Furthermore, Al3+ and Mg2+ intercalation of g-C3N4 was performed by an electrochemical method. The starting C3N4 materials and intercalation compounds were characterized by X-ray powder diffraction, Fourier transform infrared spectra, thermogravimetry, transmission electron microscopy, and X-ray photoelectron spectroscopy. The possible structure model of intercalation compounds was proposed. The cation-pi interactions and electrostatic interactions were used to explain the changes of microstructure and chemical bonds before and after intercalation.
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