Journal
JOURNAL OF MATERIALS CHEMISTRY
Volume 21, Issue 35, Pages 13283-13289Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c1jm11292a
Keywords
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Funding
- National Basic Research Program of China (973 Program) [2007CB936602, 2011CB933700]
- Anhui Normal University [2009xqn70, 2009xqn71]
- Anhui Provincial Natural Science [10040606Q34]
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Square slab-like and flower-like hydrated tungsten oxide three-dimensional architectures were synthesized by acidic precipitation of sodium tungstate solution at mild temperature. Techniques of X-ray diffraction, scanning electron microscopy, thermogravimetric-differential thermalgravimetric analysis, and transmission electron microscopy were used to characterize the structure and morphology of the products. The experimental results show that the square slab-like and flower-like WO3 center dot H2O architectures can be obtained by addition of a varying amount of 10.0 M HCl solution. The corresponding tungsten oxide three-dimensional architectures were obtained after calcinations at 400 degrees C. Finally, the obtained WO3 three-dimensional architectures were used as sensitive materials in the experiments. Compared with WO3 square slabs, the as-prepared WO3 microflowers exhibit a good response and reversibility to some organic gases, such as toluene and acetone. The responses to 100 ppm toluene and acetone are 16.7 and 17.4, respectively, at a working temperature of 320 degrees C. In addition, the sensors also exhibit a good response to ethanol, methanol and n-butanol, which indicates that the flower-like WO3 nanostructures are highly promising for applications of gas sensors.
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