Journal
JOURNAL OF MATERIALS CHEMISTRY
Volume 19, Issue 23, Pages 3914-3922Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/b902004g
Keywords
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Funding
- BMBF (Bundesministerium fur Bildung und Forschung) [01RI05028]
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Zinc oxide, aluminium oxide and binary ZnO-Al2O3 composites were synthesized using a novel preparation method that combines continuous precipitation in a microreactor with an immediate spray drying process. The sequence of the post-precipitation processes as well as the type of drying can therefore be investigated in detail and turn out to be crucial parameters to achieve high specific surface areas. By optimizing those unit operations the formation of hydrotalcite during the synthesis can be suppressed resulting in an increase of the BET surface area up to 144 m(2) g(-1) for the co-precipitated, washed, freeze-dried and subsequently calcined Zn-Al precursor.
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