Journal
JOURNAL OF MAGNETISM AND MAGNETIC MATERIALS
Volume 321, Issue 23, Pages 3921-3925Publisher
ELSEVIER
DOI: 10.1016/j.jmmm.2009.07.077
Keywords
Diphenylethene; Magnetic composite microsphere; Controlled radical polymerization
Funding
- National Natural Science Foundation of China [20374039, 50773063]
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Submicron magnetic composite microspheres have been prepared by a new surfactant free controlled radical polymerization. This new approach is based on the use of diphenylethene (DPE) as radical controlling agent and no emulsifier is required. X-ray powder diffraction (XRD), thermogravimetric analysis (TGA) and transmission electron microscopy (TEM), etc. were conducted to characterize the magnetite particles and magnetic composite microspheres. The average size of the magnetic composite microspheres prepared by this new approach is 265nm and the magnetite content of the composite microspheres is around 20%. Furthermore, the magnetic composite microspheres which surfaces have epoxy groups were also prepared. (C) 2009 Elsevier B.V. All rights reserved.
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