Journal
JOURNAL OF MAGNETIC RESONANCE
Volume 207, Issue 1, Pages 149-152Publisher
ACADEMIC PRESS INC ELSEVIER SCIENCE
DOI: 10.1016/j.jmr.2010.07.017
Keywords
Fast NMR; COSY; TOCSY; Pulsed field gradients; Triple gradients
Funding
- Integrated Infrastructure Initiative (I3) of the EC (EU-NMR) [RII3-026145]
- Centre National pour la Recherche Scientifique (CNRS) of France
- Foundation Pierre-Gilles de Gennes (PGG)
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A drastic reduction of the time required for two-dimensional NMR experiments can be achieved by reducing or skipping the recovery delay between successive experiments. Novel SMAll Recovery Times (SMART) methods use orthogonal pulsed field gradients in three spatial directions to select the desired pathways and suppress interference effects. Two-dimensional spectra of dilute amino acids with concentrations as low as 2 mM can be recorded in about 0.1 s per increment in the indirect domain. (C) 2010 Elsevier Inc. All rights reserved.
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