Journal
JOURNAL OF LABELLED COMPOUNDS & RADIOPHARMACEUTICALS
Volume 53, Issue 10, Pages 605-612Publisher
WILEY
DOI: 10.1002/jlcr.1791
Keywords
flavan-3-ol; [2-C-13, 4-C-13]-(2R, 3S)-catechin; [2-C-13, 4-C-13]-(2R, 3R)-epicatechin; CH3 (CN)-C-13; (Me2NCHO)-C-13
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The first synthesis of doubly labeled, [2-C-13, 4-C-13]-(2R,3S)-catechin 15 and [2-C-13, 4-C-13]-(2R,3R)-epicatechin 18 starting from labeled 2-hydroxy-4, 6-bis(benzyloxy)acetophenone 3 and labeled 3, 4-bis(benzyloxy)-benzaldehyde 7 are described.
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