Journal
ORGANIC PROCESS RESEARCH & DEVELOPMENT
Volume 19, Issue 9, Pages 1274-1281Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.oprd.5b00160
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Funding
- Irish Research Council for Science Engineering and Technology (IRCSET) [RS/2010/2812, EPSPG/2011/243, EPSPG/2012/741]
- Science Foundation Ireland (SFI) [11/TIDA/B2032]
- Science Foundation Ireland (SFI) [11/TIDA/B2032] Funding Source: Science Foundation Ireland (SFI)
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Herein is reported the development of a new process to manufacture (S)-pregabalin. The method comprises six steps, run under the catalysis of a recyclable polymer bound phase transfer catalyst, and afforded (S)-pregabalin in overall 54% yield, starting from building blocks acetylacetone, isovaleraldehyde, and nitromethane.
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