Journal
ORGANIC LETTERS
Volume 17, Issue 15, Pages 3646-3649Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.5b01393
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Funding
- Natural Science Foundation of Jiangsu Province of China [L210903913]
- Soochow University [Q410901212]
- Young National Natural Science Foundation of China [21402133]
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Palladium-catalyzed direct ortho-silylation of oxalyl amide-protected phenylmethanamine and phenethylamine with commercially available disilanes is reported. Germanylation products were also produced under the same reaction conditions. This protocol tolerated oxalyl amide-protected aliphatic, amines, which gave gamma-C-H silylation products.
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