Journal
ORGANIC LETTERS
Volume 17, Issue 9, Pages 2046-2049Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.5b00122
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Funding
- National Natural Science Foundation of China [21202095, 21172139, 21271125]
- Program for Science & Technology Innovation Talents in Universities of Henan Province [14HASTIT016]
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The palladium-catalyzed enantioselective intramolecular C-H arylation of N-(2-haloaryl)-P,P-diphenylphosphinic amides furnishes P-stereogenic phosphine oxide derivatives in 61-99% yield with 88-97% ee. The catalyst generated in situ from a TADDOL-derived phosphoramide ligand and Pd(dba)(2) is optimum in terms of yield and enantioselectivities.
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