Journal
ORGANIC LETTERS
Volume 18, Issue 1, Pages 112-115Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.5b03346
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Funding
- Japan Society for the Promotion of Science (JSPS) [25282228, 23102016]
- Grants-in-Aid for Scientific Research [23102016, 25282228] Funding Source: KAKEN
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Synthesis of four diastereomers of the C1-C12 fragment of amphirionin-5 has been achieved in a convergent and stereodivergent manner. Detailed comparison of the H-1 and C-13 NMR data of each compound with those reported for the natural product led to not only the stereochemical assignment of the relative configuration of the C4/C5 stereogenic centers but also reassignment of the proposed relative configuration at C9 of amphirionin-5.
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